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Vladimir K. Michaelis (editor) - Handbook of High Field Dynamic Nuclear Polarization

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Addresses Dynamic Nuclear Polarization (DNP) as a technique for sensitivity-enhancement in solid-state NMR spectroscopy

This comprehensive handbook is a compendium of the current state-of-the art of high field Dynamic Nuclear Polarizationfrom long-proven, early developments, up to todays hot topics. It covers all the relevant subjects that have made a direct or indirect contribution toward advancing this field, and focuses on topics such as: the theory behind the effects seen within DNP; instrumentation required for carrying out DNP; and specific applications of DNP including protein monitoring, catalysis, nanoparticles, biological and clinical studies. Development and application of techniques that have indirectly contributed to advancing MAS DNP NMR, such as DNP experiments on static solids within microwave resonant structures, and high-field EPR, are also examined.

Handbook of High Field Dynamic Nuclear Polarization is presented in three sectionsTheoretical Aspects, DNP Development (instrumentation / radical / sample), and DNP NMR Applications. The first section offers chapters on; solid and cross effect DNP; thermal mixing; Overhauser; and dissolution DNP. The second looks at: microwave technology, gyrotron, and IOE; homebuilt and commercial DNP spectrometers; and glassing vs. solvent-free DNP. The final section provides information on; amyloid, membrane, and nanocrystalline proteins; metals, and surface enhanced DNP; pharmaceuticals; nanoparticles; and much more.

  • Covers one of the biggest developing fields in magnetic resonance
  • Relevant to students, academics, and industry within the physical, materials, medical, and biochemical sciences
  • An excellent starting point and point-of-reference for researchers in the field
  • Edited by a widely respected team with contributions from key researchers in the NMR community
  • Part of the eMagRes Handbook Series

Handbook of High Field Dynamic Nuclear Polarization is an ideal reference for all researchers and graduate students involved in this complex, interdisciplinary field.

About eMagRes Handbooks

eMagRes publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles. In consultation with the eMagRes Editorial Board, the eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of eMagRes at your fingertips!

Visit: www.wileyonlinelibrary.com/ref/eMagRes

Vladimir K. Michaelis (editor): author's other books


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Table of Contents List of Tables Chapter 12 Chapter 20 Chapter 21 List - photo 1
Table of Contents
List of Tables
  1. Chapter 12
  2. Chapter 20
  3. Chapter 21
List of Illustrations
  1. Chapter 1
  2. Chapter 2
  3. Chapter 3
  4. Chapter 4
  5. Chapter 5
  6. Chapter 6
  7. Chapter 7
  8. Chapter 8
  9. Chapter 9
  10. Chapter 10
  11. Chapter 11
  12. Chapter 12
  13. Chapter 13
  14. Chapter 14
  15. Chapter 15
  16. Chapter 16
  17. Chapter 17
  18. Chapter 18
  19. Chapter 19
  20. Chapter 20
  21. Chapter 21
  22. Chapter 22
Guide
Pages
eMagRes Books

eMagRes (formerly the Encyclopedia of Magnetic Resonance) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of eMagRes Books handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of eMagRes articles.

Published eMagRes Books
NMR CrystallographyNMR Spectroscopy: A Versatile Tool for Environmental Research
Edited by Robin K. Harris, Roderick E. Wasylishen,Edited by Myrna J. Simpson, AndrJ. Simpson
Melinda J. DuerISBN 9781118616475
ISBN 9780470699614
Multidimensional NMR Methods for the Solution StateNMR in Pharmaceutical Sciences
Edited by Gareth A. Morris, James W. EmsleyEdited by Jeremy R. Everett, Robin K. Harris, John C. Lindon,
ISBN 9780470770757Ian D. Wilson
ISBN 9781118660256
SolidState NMR Studies of BiopolymersHandbook of Magnetic Resonance Spectroscopy In Vivo:
Edited by Ann E. McDermott, Tatyana PolenovaMRS Theory, Practice and Applications
ISBN 9780470721223Edited by Paul A. Bottomley, John R.~Griffiths
ISBN 9781118997666
NMR of Quadrupolar Nuclei in Solid MaterialsEPR Spectroscopy: Fundamentals and Methods
Edited by Roderick E. Wasylishen, Sharon E. Ashbrook,Edited by Daniella Goldfarb, Stefan Stoll
Stephen WimperisISBN 9781119162995
ISBN 9780470973981
RF Coils for MRIHandbook of High Frequency Dynamic Nuclear Polarization NMR
Edited by John T. Vaughan, John R. Griffiths
ISBN 9780470770764Edited by Vladimir Michaelis, Robert G. Griffin,
Bjrn Corzilius, Shimon Vega
ISBN 9781119441649
MRI of Tissues with Short T2s or T2s
Edited by Graeme M. Bydder, Gary D. Fullerton,
Ian R. Young
ISBN 9780470688359
Forthcoming eMagRes Books

Handbook of Safety and Biological Aspects in MRI

Edited by Devashish Shrivastava, John T. Vaughan

ISBN 9781118821305

eMagRes Edited by Sharon Ashbrook Bella Bode George A Gray John R - photo 2
eMagRes

Edited by Sharon Ashbrook, Bella Bode, George A. Gray, John R. Griffiths, Tatyana Polenova, Roberta Pieratelli, Thomas Prisner, Andr J. Simpson, Myrna J. Simpson.

eMagRes (formerly the Encyclopedia of Magnetic Resonance) is based on the original publication of the Encyclopedia of Nuclear Magnetic Resonance, first published in 1996 with an updated volume added in 2000. The Encyclopedia of Magnetic Resonance was launched in 2007 online with all the existing published material, and was later relaunched as eMagRes in 2013. eMagRes captures every aspect of the interdisciplinary nature of magnetic resonance, providing all the essential information on the science, methodologies, engineering, technologies, applications, and the history of magnetic resonance, whilst encompassing a whole range of techniques, including MRI, MRS, NMR, and EPR/ESR.

For more information see: http://www.wileyonlinelibrary.com/ref/eMagRes.

Handbook of High Field Dynamic Nuclear Polarization

Editors
Vladimir K. Michaelis
University of Alberta, Edmonton, Alberta, Canada

Robert G. Griffin
Massachusetts Institute of Technology, Cambridge, MA, USA

Bjrn Corzilius
University of Rostock, Rostock, Germany

Shimon Vega
Weizmann Institute of Science, Rehovot, Israel

Copyright This edition first published 2020 2020 John Wiley Sons Ltd - photo 3

Copyright

This edition first published 2020

2020 John Wiley & Sons Ltd

Registered Office

John Wiley & Sons Ltd, The Atrium, Southern Gate, Chichester, West Sussex,

PO19 8SQ, UK

The right of the authors to be identified as the authors of this work has been asserted in accordance with law.

All rights reserved. No part of this publication may be reproduced, stored in a retrieval system, or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, except as permitted by law.

Advice on how to obtain permission to reuse material from this title is available at http://www.wiley.com/go/permissions.

Wiley also publishes its books in a variety of electronic formats and by printondemand. Some content that appears in standard print versions of this book may not be available in other formats.

Limit of Liability/Disclaimer of Warranty: While the publisher and authors have used their best efforts in preparing this work, they make no representations or warranties with respect to the accuracy or completeness of the contents of this work and specifically disclaim all warranties, including without limitation any implied warranties of merchantability or fitness for a particular purpose. No warranty may be created or extended by sales representatives, written sales materials, or promotional statements for this work. The fact that an organization, website, or product is referred to in this work as a citation and/or potential source of further information does not mean that the publisher and authors endorse the information or services the organization, website, or product may provide or recommendations it may make. This work is sold with the understanding that the publisher is not engaged in rendering professional services. The advice and strategies contained herein may not be suitable for your situation. You should consult with a specialist where appropriate. Further, readers should be aware that websites listed in this work may have changed or disappeared between when this work was written and when it is read. Neither the publisher nor authors shall be liable for any loss of profit or any other commercial damages, including but not limited to special, incidental, consequential, or other damages.

Library of Congress Cataloging-in-Publication Data is available for this title.

9781119441649 (hardback)

A catalogue record for this book is available from the British Library.

Cover Design: Wiley

Cover Images: Courtesy of Alessandra Lucini Paioni, Marie A.M. Renault and

Marc Baldus; Courtesy of Marina Bennati and Tomas Orlando; Courtesy of

Guy M. Bernard and Vladimir K. Michaelis; Background Kjpargeter/Shutterstock

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