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Ya Wei - Mechanical Properties of Cementitious Materials at Microscale

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Ya Wei Mechanical Properties of Cementitious Materials at Microscale
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This book provides information on characterizing the microstructure and mechanical properties of cementitious materials at microscale. Specifically, with the intention to provide the methods of preparing the samples for the micro-scale mechanical testing, to address the techniques for measuring and analyzing the elastic modulus, the stiffness, and the fracture toughness of cementitious materials at micro scale by instrumented indentation, to describe a method for measuring and interpreting creep behavior of cementitious materials at micro scale, and to demonstrate the homogenization method for obtaining the mechanical properties of cementitious materials across scales. The information in this book is helpful to a wide readership in the field of civil engineering and materials science working with cementitious materials and other composite materials.

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Book cover of Mechanical Properties of Cementitious Materials at Microscale - photo 1
Book cover of Mechanical Properties of Cementitious Materials at Microscale
Ya Wei , Siming Liang and Weikang Kong
Mechanical Properties of Cementitious Materials at Microscale
The Springer logo Ya Wei Department of Civil Engineering Tsinghua - photo 2

The Springer logo.

Ya Wei
Department of Civil Engineering, Tsinghua University, Beijing, China
Siming Liang
School of Civil Engineering, Sun Yat-sen University, Guangzhou, China
Weikang Kong
Department of Civil Engineering, Tsinghua University, Beijing, China
ISBN 978-981-19-6882-2 e-ISBN 978-981-19-6883-9
https://doi.org/10.1007/978-981-19-6883-9
The Editor(s) (if applicable) and The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2023
This work is subject to copyright. All rights are solely and exclusively licensed by the Publisher, whether the whole or part of the material is concerned, specifically the rights of translation, reprinting, reuse of illustrations, recitation, broadcasting, reproduction on microfilms or in any other physical way, and transmission or information storage and retrieval, electronic adaptation, computer software, or by similar or dissimilar methodology now known or hereafter developed.
The use of general descriptive names, registered names, trademarks, service marks, etc. in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use.
The publisher, the authors, and the editors are safe to assume that the advice and information in this book are believed to be true and accurate at the date of publication. Neither the publisher nor the authors or the editors give a warranty, expressed or implied, with respect to the material contained herein or for any errors or omissions that may have been made. The publisher remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

This Springer imprint is published by the registered company Springer Nature Singapore Pte Ltd.

The registered company address is: 152 Beach Road, #21-01/04 Gateway East, Singapore 189721, Singapore

To Jiren, Jiyuan, Liangchun, Yulan, Dewei, and Xiaohong.

Preface

The measurement of micro scale mechanical properties of cementitious materials has gained interest in the last one to two decades. This book grows out of the ten years of research work by the authors in this area, with the intention to (1) provide the methods of preparing the samples for the micro scale mechanical testing, (2) address the techniques for measuring and analyzing the elastic modulus, the stiffness, and the fracture toughness of cementitious materials at micro scale by instrumented indentation, (3) describe a method for measuring and interpreting creep behavior of cementitious materials at micro scale, and (4) demonstrate the homogenization method for obtaining the mechanical properties of cementitious materials across scales.

This book is designed primarily for use at the undergraduate level, but it can also serve as a guide for professionals working with cementitious materials and other composite materials. The information in this book is illustrated by large amounts of figures, tables, text, and the references, which is helpful to a wide readership in the various fields of civil engineering and materials science. Although we have cited and compiled a list of references that we believe are most relevant to the text, listing such a limited number of references does not represent the breadth and depth of this field. We sincerely apologize to those authors whose works were not cited.

Finally, we would like to express our gratitude to our students and colleagues at Tsinghua University for their valuable input and collaboration. This book would not have been completed without the supports from our families; this book is dedicated to them.

Ya Wei
Weikang Kong
Siming Liang
Beijing, China Beijing, China Guangzhou, China
Abbreviations
a/c ratio

Aggregate-to-cement ratio

AFM

Atomic force microscope

AFm

Monosulfate

Aft

Ettringite

AGG

Aggregate

BSE

Backscattered electron

C2S

Dicalcium silicate

C3A

Tricalcium aluminate

C3S

Tricalcium silicate

C4AF

Tetracalcium aluminoferrite

CASH

Calcium aluminum silicate hydrate

CDF

Cumulative distribution function

CH

Calcium hydroxide (or portlandite)

CL

Clinker

CNTs

Carbon nanotubes

COF

Coefficient of friction

CSH

Calcium silicate hydrate

CSM

Continuous stiffness measurement

CTOD

Crack tip opening displacement

DOH

Degree of hydration

DT

Differential

EDS

Energy-dispersive X-ray spectroscopy

EM

ExpectationMaximization

EMI

Effective mixed interphase

FEA

Finite element analysis

FEM

Finite element method

FFT

Fast Fourier transform

FIB

Focused ion beam

FT

Freezethaw cycles

GEM

General effective media

GSC

Generalized self-consistent

HD CSH

High-density calcium silicate hydrate

HP

Hydration product

IDD

Interaction direct derivative

IP

Inner product

ITZ

Interfacial transition zone

K-T

KatzThompson equation

LD CSH

Low-density calcium silicate hydrate

LEM

LawnEvansMarshall method

LVDT

Linear voltage displacement transducer

MI

Microindentation

MIP

Mercury intrusion porosimetry

MLE

Maximum likelihood estimation

MT

MoriTanaka

N2-BET

N2 BrunauerEmmettTeller nitrogen gas adsorption

NI

Nanoindentation

NMR

Nuclear magnetic resonance

NS

Nanosilica

OP

Outer product

OPC

Ordinary Portland cement

PDF

Probability density function

RAC

Recycled aggregate concrete

RH

Relative humidity

RVE

Representative volume element

SC

Self-consistent

SE

Secondary electron

SEM

Scanning electron microscope

SPM

Scanning probe microscopy

TGA

Thermal gravimetric analyzer

TXM

Transmission X-ray microscope

UHD CSH

Ultrahigh-density calcium silicate hydrate

UHPC

Ultrahigh-performance concrete

w/b ratio

Water-to-binder ratio

w/c ratio

Water-to-cement ratio

w/cm ratio

Water-to-cementitious ratio

X-ray CT

X-ray computed tomography

Contents
The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2023
Y. Wei et al. Mechanical Properties of Cementitious Materials at Microscale https://doi.org/10.1007/978-981-19-6883-9_1
1. Introduction
Ya Wei
(1)
Department of Civil Engineering, Tsinghua University, Beijing, China
(2)
School of Civil Engineering, Sun Yat-sen University, Guangzhou, China
(3)
Department of Civil Engineering, Tsinghua University, Beijing, China
Ya Wei (Corresponding author)
Email:
Siming Liang
Email:
Weikang Kong
Email:
Abstract

Currently, cementitious materials have become the most widely-used civil engineering materials around the world, which have been used to construct concrete structures such as buildings, dams, tunnels, bridges, and roads, etc.

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